High Pressure Oxygen Tube Furnace with 20mm ID up to 1100C @ 610PSI - OTF1200XHP55

OTF-1200X-HP-55 is a split tube furnace with a Ni-based super-alloy tube (55mm O.D x 20 mm I.D x 600 mm L) and valves. It is designed for use at high pressure (7 MPa) up to 1100°C under oxidizing and inert gas atmospheres to process special compounds. It is an ideal furnace to use for preparing new materials under high pressure and can also be used as a mini HIP to treat metallic samples. ( Laptop is included since 9/10/15 )

SPECIFICATIONS

Furnace Structure	Double-layer steel casing with air cooling. High-purity fibrous alumina insulation for max. energy saving. The aluminum heat sink on the processing tube to ensure pressure flange and fitting < 80°C The processing tube is made of Ni-based super-ally
Power	2.5KW
Voltage	AC 208 - 240V Single Phase, 50/60 Hz
Max. Temperature	1100°C
Max. Heating Rate	<= 30°C/min
Continuous Heating Temperature	RT-1000°C
Material and Size of Pressure Vessel	Special Ni-based Superalloy: ( Waspaloy or equivalent ) 55 mm O.D x 20 mm I.D. x 580 mm Length  1/4BSPP fitting is installed at the end of the flange, and 1/4" high-pressure stainless steel pipe shall be connected to the fitting. Please click the picture below to see the details of the pressure vessel ExteriorInterior Warning: Never put a sample inside the tube directly without a crucible or isolated foil to avoid the sample reacting with the tube alloy. Attention: The processing Tube is a consumable part, you can click the picture below to order a replacement or a spare one. Copper Gasket Size: 27.2mm O.D x 20mm I.D x 2mm thickness The optional torque wrench is available here to avoid overtightening the flange bolts. The suitable tightening torque for 55 ODx 20 ID x 580 L (mm) is the 40-foot pound.
Compatible Gas and Crucible	O2 and inert gasses such as N2, Ar and He Note: A small quartz or Alumina boat shall be used to load the sample inside the vessel. Please click the link below to order separately. Never place the sample directly onto the vessel without a crucible. Vessel service life could be reduced significantly if you don't do so. You may use gold or nickel foil to wrap the crucible boat to minimize the contamination to the pressure vessel.
Heating Zone length	250 mm ( single zone )
Temperature Uniformity	Constant Temperature Zone length: 50mm within +/-1°C and  70mm within +/-2°C in Click the picture below to view the details of the Temperature Distribution Curve and Testing:           Temp. Control ( left meter )
Thermocouple	Omega 3mm OD K Type with high-temperature tolerance (220°C) connector
Temperature Control	MET certified 30 programmable segments for precise control of heating rate, cooling rate and dwell time. Built-in PID Auto-Tune function with overheating & broken thermocouple broken protection. Over-temperature protection and alarm allow for operation without attendant(s). +/- 1 ºC temperature accuracy.
PC Control	A brand new laptop with pre-installed & tested software included for immediate use.(Laptop is included since 9/10/15)  Pre-installed MTS-02 Control Software is included for controlling and displaying temperature and pressure by PC at a remote location. Please don't try to buy a furnace without a computer because of liability issues
Pressure Sensor and Display	Precision high-pressure sensor (Pressure measurement range: 0~25Mpa) installed on the pressure vessel. The pressure sensor is installed in the flange. The pressure will be displayed in the pressure controller in the front panel of the furnace. The alarm system is built into the pressure controller, which allows the user to set up the high and low limit points of pressure. When the measuring pressure exceeds the limit point, the alarm strobe and whistle will be activated for the warning. When the pressure reaches the alarm set point (Max.15Mpa), the pressure inside the vessel will be released via the solenoid valve installed on the flange. For Max. pressure >15 Mpa, please shut off the manual needle valve Optional: Adjustable High-Pressure Relief Valve 1000 - 10,000 PSI (7 - 70 Mpa), click the picture below right to order.  Pressure Display flange assembly  pressure Relief Valv
Pressure Fitting	One Super-alloy flange is included. One Aluminum heat radiators are installed in front of the flange to keep the flange below 100 A high-temperature pressure transmitter, MTI-ZQ-GW is pre-installed with a flange One solenoid valve(Max.15Mpa) is pre-installed. The safety pressure relief valve is installed on the downstream side.
Options	You may order four Pt wire ( 0.35 mm dia ) feed-throughs to install the furnace for measuring material electric conductivity under high pressure up to 1100oC at extra cost. 10 mm Sapphire window can be installed on the flange for the Ramman beam under high pressure at extra cost ( click the picture below right to see details） To measure the electric properties of thermoelectric ceramics under high pressure & temperature conditions, please order an alumina testing fixture and high-pressure electrical feedthrough (10Mpa Max.) with the furnace (additional fee will apply).
Working Pressure vs temperature	Allowable pressure (SF = 2) Heating temperature Max. 3046 PSI (21 Mpa) 800°C Max. 1813 PSI (12.5 Mpa) 900°C Max. 914 PSI (6.3 Mpa) 1000°C Max. 610 PSI (4.2 Mpa) 1100°C The allowable pressure is calculated based on Barlow's formula. S = yield strength. Safety factory= 2 Click to download the GH747 nickel-based alloy datasheet Warning:  Please set up a pressure alarm point in the digital pressure display before the operation Must install a pressure regulator on the gas cylinder to increase pressure gradually.
Heating Element	Fe-Cr-Al Alloy doped by Mo
Certificate	CE Certified NRTL or CSA certification is available at an extra cost of $3500.00
Application Notes	Hytort Application, or named Hydroretorting of Shale Oil is a process developed by IGT to double the yield of shale oil and hydrocarbon gasses. Please click underlined to view the research paper.
Safety Notes The picture shows a Ni-based Superalloy ( Waspaloy or equivalent) processing tube under an overpressure test.	Ni-based Super-alloy ( Waspaloy or equivalent) is a reliable processing tube that can be used under high temperatures and high pressure. It has excellent ductility and tensile properties so only creep deformation happens under an overpressure destruction test followed by a crack formed (usually at the hot zone at the center of the tube) to release the pressure. Brittle fracture won’t happen in the overpressure destruction test which means no tube explosion will happen under Attention: For the use of flammable, toxic or corrosive gasses, you must contact MTI engineering group for a consultation to know all the prerequisites and precautionary measures. Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure. Click here to learn about the installation of a gas regulator. Do not over-tightening the flange screws as this may cause permanent damage to the flange or screws. Please refer to the instructions about proper torque for installing CF flange bolts. We recommend you use a torque wrench to tighten the screws with the flange. Warning： Never put a sample inside the tube directly without a crucible or isolated foil to avoid sample reaction with tube alloy.